Hasan Tanak, Karataş, Şadiye Meral, Seher Ağar, Ayşen Alaman
Published in
Crystallography Reports
AbstractA novel Schiff base compound was synthesized and characterized by IR spectroscopy and X-ray diffraction method. The compound crystallizes in monoclinic space group P21/c with Z = 4 in the unit cell. The ring systems are perfectly planar but the whole molecule is not planar. The dihedral angle between the thiophene and phenyl rings is 38.7(3...
Sharma, A. Nurjamal, K. Banerjee, B. Brahmachari, G. Gupta, V. K.
Published in
Crystallography Reports
AbstractThe cyclohexene derivative 5'-amino-4,4''-dichloro-2'-nitro-2',3'-dihydro-[1,1':3',1''-terphenyl]-4',4',6'(1'H)-tricarbonitrile-dimethyl sulfoxide has been synthesised via one-pot pseudo five component reaction and its crystal structure is determined by X-ray analysis. The crystal is triclinic and its space group is P\documentclass[12pt]{mi...
Önal, M. Altıokka, B.
Published in
Crystallography Reports
AbstractLayers of zinc oxide (ZnO) on glass substrates were grown by chemical bath deposition method. This method refers to solvo-thermal methods of crystal growth. When either ethylene-diamine-tetraacetic acid (EDTA) or ammonia was used as a complex agent, very weak adhesion of ZnO nanoparticles to the surface of glass substrates was noted, and wh...
Hasan Tanak, Meral, Seher Ağar, Ayşen Alaman
Published in
Crystallography Reports
Abstract6,6'-(1E,1'E)-(ethane-1,2-diylbis(azan-1-yl-1-ylidene))bis(phenylmethan-1-yl-1-ylidene)bis(3-(octyloxy)phenol) has been synthesized and characterized by FTIR, 1H, 13C NMR and single-crystal X-ray determination. The compound crystallizes in monoclinic space group C2/c with Z = 4 in the unit cell. The asymmetric unit of the compound contains ...
Sharma, S. Brahmachari, G. Gupta, V. K.
Published in
Crystallography Reports
AbstractThe communication deals with the eco-friendly synthesis and X-ray crystal structure of an organic carbonitrile, namely 6-amino-3-phenyl-4-(pyridin-4-yl)-2,4-dihydropyrano[2,3-c]pyrazole-5-carbonitrile. The title compound was synthesized in 89% yield by following a simple, straightforward and highly efficient multicomponent one-pot protocol ...
Shashi, R. Prasad, N. L. Begum, Noor Shahina
Published in
Crystallography Reports
AbstractThiazolo[3,2-a]pyrimidines namely ethyl 2-acetyl-5-(2-fluorophenyl)-3,7-dimethyl-5H-thiazolo[3,2-a]pyrimidine-6-carboxylate 3a, ethyl 2-acetyl-5-(3-fluorophenyl)-3,7-dimethyl-5H-thiazolo[3,2-a]pyrimidine-6-carboxylate 3b, and ethyl 2-acetyl-5-(4-fluorophenyl)-3,7-dimethyl-5H-thiazolo[3,2-a]pyrimidine-6-carboxylate 3c were obtained by one po...
Lei Guan, Wang, Xin Wang, Ying
Published in
Crystallography Reports
AbstractA new lanthanide metal complex [Tm2(H2L)3(phen)2] (1) (Na2H2L = 4,5-dihydroxy-1,3-benzenedisulfonic acid disodium salt, phen = 1,10-phenanthroline) was synthesized by hydrothermal method. It has been characterized by single crystal X-ray diffraction, elemental analysis and thermogravimetric (TG) analysis. The X-ray diffraction analysis reve...
Ilyushin, G. D.
Published in
Crystallography Reports
AbstractA geometrical and topological analysis and simulation of the self-assembly of the crystal structures of intermetallic compounds formed in the K–M (M = Ag, Au, As, Sb, Bi, Ge, Sn, Pb) systems have been performed using computation methods (the ToposPro software). The precursor metal clusters of KnMm crystal structures are determined based on ...
Yi-Lin Gong, Dai, Peng Chen, Ye Ding, Shi Liu, Ju
Published in
Crystallography Reports
AbstractThe title compound C19H17F3N6 was synthesized and structurally characterized by infrared and mass spectroscopy, 1H NMR, elemental analyses and single crystal X-ray diffraction. The compound crystallizes in monoclinic system, space group P21/c with a = 17.097(4) Å, b = 7.1668(16) Å, c = 18.389(3) Å, β = 118.251(15)°, V = 1984.8(8) Å3, Z = 4,...
Pushcharovsky, D. Yu. Zubkova, N. V. Setkova, T. V. Balitskii, V. S. Nekrasov, A. N. Nesterova, V. A.
Published in
Crystallography Reports
AbstractCrystals of a (Ga,Ge)-analogue of tourmaline have been synthesized by hydrothermal method in the temperature range of 600–650°C under a pressure of 100 MPa. The composition is analyzed, and the structure of single crystals is determined by X-ray diffraction (XRD) analysis. The rhombohedral-cell parameters are found to be a = 16.0102(4) Å, c...
