Vapor-phase silylation of Al-MWW layered precursor with SiMe(2)Cl(2) and following calcination produced an interlayer-expanded MWW structure with 12-membered ring micropores without delamination as a result of the formation of silica puncheons between the MWW sheets; strong acidity of zeolitic nature was retained.
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The corresponding record at NLM can be accessed at https://www.ncbi.nlm.nih.gov/pubmed/19532897