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Three-step synthesis of Pd0/TiO2

Authors
  • Shishmakov, A. B.1
  • Mikushina, Yu. V.1
  • Petrov, L. A.1
  • 1 Ural Branch of the Russian Academy of Sciences, I. Ya. Postovsky Institute of Organic Synthesis, 22/20 ul. S. Kovalevskoi, Ekaterinburg, 620990, Russian Federation , Ekaterinburg (Russia)
Type
Published Article
Journal
Russian Chemical Bulletin
Publisher
Springer US
Publication Date
Jul 01, 2019
Volume
68
Issue
7
Pages
1451–1453
Identifiers
DOI: 10.1007/s11172-019-2576-2
Source
Springer Nature
Keywords
License
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Abstract

A simplifi ed procedure for the synthesis of Pd0/TiO2 xerogel has been developed, which includes the following steps: hydrolysis of tetrabutoxytitanium from its mixture with a palladium salt in an acetic acid atmosphere, drying and calcining the material at 860 °C. Palladium in the calcined xerogel is present in the form of spherical particles, titanium dioxide — as rutile aggregates.

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