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Spirocyclic 2,5-dihydro-1H-imidazole 1-oxyl radicals with a mesogenic substituent on C4. Synthesis and crystal structure

Authors
  • Zaytseva, E. V.1
  • Gatilov, Yu. V.1
  • Amitina, S. A.1
  • Tamura, R.2
  • Grigor’ev, I. A.1
  • Mazhukin, D. G.1, 3
  • 1 Russian Academy of Sciences, Vorozhtsov Novosibirsk Institute of Organic Chemistry, Siberian Branch, pr. Akademika Lavrent’eva 9, Novosibirsk, 630090, Russia , Novosibirsk (Russia)
  • 2 Kyoto University, Graduate School of Human and Environmental Studies, Kyoto, 606-8501, Japan , Kyoto (Japan)
  • 3 Novosibirsk State University, ul. Pirogova 2, Novosibirsk, 630090, Russia , Novosibirsk (Russia)
Type
Published Article
Journal
Russian Journal of Organic Chemistry
Publisher
Springer US
Publication Date
Jan 01, 2014
Volume
50
Issue
1
Pages
72–77
Identifiers
DOI: 10.1134/S107042801401014X
Source
Springer Nature
Keywords
License
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Abstract

Stable spirocyclic 2,5-dihydro-1H-imidazole 1-oxyl radicals containing a mesogenic fragment were synthesized on the basis of 1-[4-hydroxy(alkoxy)phenyl]-2-hydroxyamino-2-methylpropan-1-ones. The crystalline structure of two aminoxyl radicals was determined by X-ray analysis.

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