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Simultaneous determination of flubendiamide its metabolite desiodo flubendiamide residues in cabbage, tomato and pigeon pea by HPLC.

Authors
  • Paramasivam, M
  • Banerjee, Hemanta
Type
Published Article
Journal
Bulletin of Environmental Contamination and Toxicology
Publisher
Springer-Verlag
Publication Date
Oct 01, 2011
Volume
87
Issue
4
Pages
452–456
Identifiers
DOI: 10.1007/s00128-011-0389-6
PMID: 21858703
Source
Medline
License
Unknown

Abstract

A sensitive and simple method for simultaneous analysis of flubendiamide and its metabolite desiodo flubendiamide in cabbage, tomato and pigeon pea has been developed. The residues were extracted with QuEChERS method followed by dispersive solid-phase extraction with primary secondary amine sorbent to remove co extractives, prior to analysis by HPLC coupled with UV-Vis detector. The recoveries of flubendiamide and desiodo flubendiamide were ranged from 85.1 to 98.5% and 85.9 to 97.1% respectively with relative standard deviations (RSD) less than 5% and sensitivity of 0.01 μg g(-1). The method offers a less expensive and safer alternative to the existing residue analysis methods for vegetables.

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