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NOTIZEN: 2-Trifluoroacetyl-1-methyl-1, 2,3,4- tetrahydro-β-carboline, a Gaschromatographically Useful Derivative of the Mammalian Alkaloid Eleagnine

Authors
  • Peters, Karl
  • Peters, Eva-Maria
  • Bringmann, Gerhard
  • God, Ralf
Type
Published Article
Journal
Zeitschrift für Naturforschung B
Publisher
Verlag der Zeitschrift für Naturforschung
Publication Date
Oct 01, 1995
Volume
50
Issue
10
Pages
1564–1565
Identifiers
DOI: 10.1515/znb-1995-1022
Source
De Gruyter
Keywords
License
Green

Abstract

The title compound was prepared by N -trifluoroacetylation of 1-methyl-1,2,3,4-tetrahydro- β-carboline (eleagnine, 3) using trifluoroacetic anhydride. It crystallizes from methanol in the orthorhombic system, space group Pbca; a = 1334.5(2), b = 1587.0(2) and c = 1237.5(1) pm. In the crystal the molecules are connected via hydrogen bonding to form zigzag chains parallel [001],

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