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Preparation of azulenyllithium and magnesium reagents utilizing halogen–metal exchange reaction of several iodoazulenes with organolithium or magnesium ate complex

Authors
Journal
Tetrahedron Letters
0040-4039
Publisher
Elsevier
Publication Date
Volume
45
Issue
14
Identifiers
DOI: 10.1016/j.tetlet.2004.02.059
Keywords
  • Azulene
  • Organolithium
  • Organomagesium Ate Complex
  • Halogen–Metal Exchange Reaction
  • Nucleophilic Reaction

Abstract

Abstract Preparation of several azulenyllithium and magnesium reagents was achieved by the halogen–metal exchange reaction of iodoazulenes with n-butyllithium or lithium tri( n-butyl)magnesate at low temperature and the synthetic application of the reagents was explored.

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