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Synthesis of activated disulfide adducts containing a 4-diazocyclohexa-2,5-dienone precursor for photoaffinity labelling

Authors
Journal
Tetrahedron Letters
0040-4039
Publisher
Elsevier
Publication Date
Volume
35
Issue
51
Identifiers
DOI: 10.1016/0040-4039(94)88510-9
Disciplines
  • Design

Abstract

Activated disulfides 7a/b, precursors of corresponding 4-diazocyclohexa-2,5-dienones, were designed for covalent but reversible binding to cysteine containing peptides and were synthesized from 1a/b in 49 / 66 % overall yield.

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