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Complete analysis of the 1H- and 13C-NMR spectra of four blood-group A active oligosaccharides.

Authors
  • Strecker, G
  • Wieruszeski, J M
  • Michalski, J C
  • Montreuil, J
Type
Published Article
Journal
Glycoconjugate journal
Publication Date
Jan 01, 1989
Volume
6
Issue
3
Pages
271–284
Identifiers
PMID: 2535489
Source
Medline
License
Unknown

Abstract

The fully assigned 1H and 13C-NMR spectra of four group A oligosaccharides by use of multiple-relayed, coherence-transfer chemical-shift-correlated spectroscopy (multiple-RELAY-COSY) and 1H-/13C-correlation spectroscopy are reported. These analyses were performed on the following compounds: III-A; GalNAc alpha 1-3[Fuc alpha 1-2]Gal: VI-A; GalNAc alpha 1-3[Fuc alpha 1-2]Gal beta 1-3[Fuc alpha 1-4]GlcNAc beta 1-3Gal: VII-A-1; GalNAc alpha 1-3[Fuc alpha 1-2]Gal beta 1-3[Fuc alpha 1-4]GlcNAc beta 1-3Gal beta 1-1Glycerol: VII-A-2; GalNAc alpha 1-3[Fuc alpha 1-2]Gal beta 1-3[Fuc alpha 1-4]GlcNAc beta 1-3Gal beta 1-4Glc.

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