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Preparation of the phosphonic acid analogue of 3-deoxy-D-manno-2-octulosonic acid (KDO)

Authors
Journal
Tetrahedron Letters
0040-4039
Publisher
Elsevier
Publication Date
Volume
37
Issue
10
Identifiers
DOI: 10.1016/0040-4039(96)00075-5

Abstract

A phosphonic acid analogue synthesis of KDO is described using in the key step a lithiated anion derived from diethyl 1,3-dithiacyclohexylphosphonate as an efficient synthetic equivalent to install an α-ketophosphonate unit onto a conveniently protected D-mannitol triflate

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