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Catalytic thiomethylation of regioisomeric aminobenzamides using bis(N,N-dimethylamino)methane and α,ω-alkanedithiols

Authors
  • Khairullina, R. R.1
  • Tyumkina, T. V.1
  • Ibragimov, A. G.1
  • 1 Russian Academy of Sciences, 141 prosp. Oktyabrya, Bashkortostan, Ufa, 450075, Russian Federation , Ufa (Russia)
Type
Published Article
Journal
Russian Chemical Bulletin
Publisher
Springer US
Publication Date
Apr 01, 2021
Volume
70
Issue
4
Pages
757–762
Identifiers
DOI: 10.1007/s11172-021-3147-x
Source
Springer Nature
Keywords
License
Yellow

Abstract

A chemoselective synthesis of acyclic and cyclic S-containing aminobenzamides was developed. The method involved samarium-catalyzed thiomethylation of regioisomeric aminobenzamides at the amino group using either bis(N,N-dimethylamino)methane and α,ω-alkanedithiols or bis-1,3-aminosulfides.

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