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A simple method to prepare unsymmetrical di- tri- and tetrasulfides

Authors
Journal
Tetrahedron Letters
0040-4039
Publisher
Elsevier
Publication Date
Volume
35
Issue
30
Identifiers
DOI: 10.1016/s0040-4039(00)73505-2

Abstract

Unsymmetrical di- tri- and tetrasulfides can be prepared in a one-pot reaction using SO 2Cl 2, SCl 2 and S 2Cl 2 respectively to permit coupling of the appropriate thiols. Yields of isolated, pure product range from 25%-quantitative.

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