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A flow-microcalorimetric vessel for solution of slightly soluble solids

Authors
Journal
The Journal of Chemical Thermodynamics
0021-9614
Publisher
Elsevier
Publication Date
Volume
18
Issue
12
Identifiers
DOI: 10.1016/0021-9614(86)90160-6
Disciplines
  • Design

Abstract

Abstract A flow-calorimetric vessel has been designed for the determination of enthalpies of solution for slightly soluble solids with particular reference to water as a solvent. The design was chosen to fit a 2277 multi-channel microcalorimeter system, LKB Products, Bromma, Sweden. At each experiment the ampoule was charged with 1 to 10 mg of the solid substance. The instrument has been tested by solution of acetanilide and adenine in water in the temperature ranges 288 to 310 K and 288 to 318 K, respectively.

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