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Vibrational spectra ofM(CC-CH3)4withM= Si, Ge or Pb andM(CC-CH3)3, withM= P, As or Sb

Authors
Journal
Spectrochimica Acta Part A Molecular Spectroscopy
0584-8539
Publisher
Elsevier
Publication Date
Volume
28
Issue
7
Identifiers
DOI: 10.1016/0584-8539(72)80106-5

Abstract

Abstract Infrared spectra of M(CC-CH 3) 4 ( M = Si, Ge, Pb) and M(CC-CH 3) 3 ( M = P, As, Sb) have been measured from 33 to 4000 cm −1 as solids dispersed in KBr and Nujol and as solutions in CCl 4 and CS 2 (and as a vapor for As(CC-CH 3) 3 only). Raman spectra were measured in the solid state and for solutions in several solvents. Polarizations were obtained in solution. T d symmetry was assumed for M(CC-CH 3) 4 and C 3 v for M(CC-CH 3) 3 and was completely satisfactory. Most of the spectroscopically active fundamentals could be assigned with little difficulty.

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