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An unusual reaction of azide with nitroolefins

Authors
Journal
Tetrahedron Letters
0040-4039
Publisher
Elsevier
Publication Date
Volume
20
Issue
50
Identifiers
DOI: 10.1016/s0040-4039(01)86731-9

Abstract

Abstract The reaction of sodium azide in DMSO with 9-dinitromethylenefluorene (DNF) and 9-bromonitromethylenefluorene (BNF) results in the formation of N-cyano-9-iminofluorene ( 2 ). The overall reaction time is two minutes at room temperature.

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