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First total synthesis of 6-tuliposide B

Authors
Publisher
Elsevier Ltd
Publication Date
Volume
19
Issue
12
Identifiers
DOI: 10.1016/j.tetasy.2008.05.019

Abstract

Abstract Labile (+)-6-tuliposide B, an antimicrobial compound produced by tulip, was synthesized in nine steps from d-glucose via the Baylis–Hillman reaction of 2-( tert-butyldimethylsilyloxy)-acetaldehyde with 6- O-acryloyl-1- O-(2-trimethylsilylethyl)-β- d-glucopyranoside, followed by a mild deprotection procedure using TFA in CH 2Cl 2.

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