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Synthesis, X-ray structure and high-resolution NMR spectroscopy of methyl 3-azido-2,3-dideoxy-α-d-arabino-hexopyranoside

Authors
Journal
Carbohydrate Research
0008-6215
Publisher
Elsevier
Publication Date
Volume
323
Identifiers
DOI: 10.1016/s0008-6215(99)00274-8
Keywords
  • Methyl 3-Azido-2
  • 3-Dideoxy-α-D-Arabino-Hexopyranoside
  • Synthesis
  • X-Ray Diffraction
  • Methyl 4
  • 6-Di-O-Acetyl-3-Azido-2
  • 3-Dideoxy-α-D-Arabino-Hexopyranoside
  • 1H And13C Nmr

Abstract

Abstract The synthesis, crystal structure data and 1H and 13C NMR spectroscopy of methyl 3-azido-2,3-dideoxy-α- d- arabino-hexopyranoside ( 5b) is reported. This compound adopts the 4 C 1 conformation. Hydrogen-bonded molecules of 5b form helices around the crystallographic 4 1 axis.

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