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Präparative und I.R.-spektroskopische untersuchungen zur umsetzung von P3N3Br6und P3N3Cl6mit dimethylamin

Authors
Journal
Journal of Inorganic and Nuclear Chemistry
0022-1902
Publisher
Elsevier
Publication Date
Volume
29
Issue
4
Identifiers
DOI: 10.1016/0022-1902(67)80079-4

Abstract

Abstract Details on the preparation of P 3N 3Br 5[N(CH 3) 2], cis-, trans-, and gem.-P 3N 3Br 4[N(CH 3) 2] 2 and trans- and gem.-P 3N 3Br 3[N(CH 3) 2] 3 are given. These substances (including some Cl-analogs) are documented by their i.r.-spectra between 400 and 4000 cm −1 and by their X-ray diffraction data. Compounds of this type with 4 and 5 N(CH 3) 2-groups are shown to exist in mixtures.

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