Affordable Access

Publisher Website

Synthesis and characterization of AlPO4-36: a novel aluminophosphate molecular sieve with ATS structure

Authors
Journal
Microporous and Mesoporous Materials
1387-1811
Publisher
Elsevier
Publication Date
Volume
32
Issue
3
Identifiers
DOI: 10.1016/s1387-1811(99)00110-9
Keywords
  • 27Al And31P Mas Nmr
  • Alpo-36
  • Ats Structure Type
  • Molecular Sieves
  • Scanning Electron Microscopy
  • Xps
  • Xrd
Disciplines
  • Chemistry
  • Earth Science
  • Geography

Abstract

Abstract AlPO-36, the parent member of the ATS molecular sieve structure type, has been synthesized hydrothermally from gels containing only Al and P oxides. Four series of syntheses were carried out to determine the best conditions for the preparation of AlPO-36 free of AlPO-H3. Characterization of the synthesis products was performed using X-ray diffraction (XRD), chemical analysis, scanning electron microscopy (SEM), N 2 adsorption, X-ray photoelectron spectroscopy (XPS) and 27Al and 31P MAS NMR. X-ray powder diffraction patterns are comparable to those previously reported for MAPO-36.

There are no comments yet on this publication. Be the first to share your thoughts.