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Polyhydrate 1,10-Diaza-18-crown-6·8.25H2O

Authors
Journal
Mendeleev Communications
0959-9436
Publisher
Elsevier
Publication Date
Volume
5
Issue
6
Identifiers
DOI: 10.1070/mc1995v005n06abeh000545

Abstract

The phase diagram of the system 1,10-diaza-18-crown-6–H 2O has been studied; polyhydrate 1,10-diaza-18-crown-6-8.25H 2O, which melts incongruently at 16.0 °C, has been found in this system. Each cavity of the three-dimensional framework made of water molecules accommodates four molecules of crown ether; the hydrate has the following crystallographic parameters: a = 18.848(2), c= 13.159(2) Å ( T = −100°C), space group P4 2/n and Z = 8.

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