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A versatile radical based approach toO-alkylated hydroxylamines and oximes

Authors
Journal
Tetrahedron
0040-4020
Publisher
Elsevier
Publication Date
Volume
64
Issue
52
Identifiers
DOI: 10.1016/j.tet.2008.08.113

Abstract

Abstract O-Alkylhydroxylamines, often used for the preparation of bioconjugates, can be readily obtained by radical addition to suitable O-alkenylhydroxylamine derivatives. In the case of N-Boc- O-allylhydroxylamine, the addition is unexpectedly followed by elimination resulting in an overall allylation of the radical species.

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