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A convenient synthesis of glycals employingin-situgenerated Cp2TiCl

Authors
Journal
Tetrahedron Letters
0040-4039
Publisher
Elsevier
Publication Date
Volume
40
Issue
33
Identifiers
DOI: 10.1016/s0040-4039(99)01266-6

Abstract

Abstract Reductive elimination of acetylated glycosyl bromides to the corresponding glycal is easily achieved by mixing the bromide with Cp 2TiCl 2 and Mn in THF, and hence does not require the separate preparation of Cp 2TiCl using glove-box techniques.

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