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Thermal analysis of bis(tetraethylammonium) tetrachloroferrate(II)

Authors
Journal
Thermochimica Acta
0040-6031
Publisher
Elsevier
Publication Date
Volume
480
Identifiers
DOI: 10.1016/j.tca.2008.09.022
Keywords
  • Tetrahalogenoferrates(Ii)
  • Thermal Decomposition
  • Mössbauer Spectroscopy

Abstract

Abstract Thermal decomposition of bis(tetraethylammonium) tetrachloroferrate(II) has been studied using the TG-FTIR, TG–MS and DTA techniques. The measurements were carried out in an inert atmosphere over the temperature range of 293–1073 K. The solid products of the thermal decomposition were identified by the FT-FIR, Mössbauer spectroscopy as well as the X-ray powder diffractometry. The influence of the oxidation state and the nature of a metal on thermal transformation profiles of analogous complexes have been discussed.

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