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(E)-N′-(3,4-Dimethoxy­benzyl­idene)-2,4-dihydroxy­benzohydrazide methanol solvate

Authors
Journal
Acta Crystallographica Section E Structure Reports Online
1600-5368
Publisher
International Union of Crystallography
Publication Date
Volume
65
Issue
10
Identifiers
DOI: 10.1107/s1600536809035752
Keywords
  • Organic Papers

Abstract

The title compound, C16H16N2O5·CH3OH, was obtained from a condensation reaction of 3,4-dimethoxy­benzaldehyde and 2,4-dihydroxy­benzohydrazide. The non-H atoms of the Schiff base mol­ecule are approximately coplanar (r.m.s. deviation = 0.043 Å) and the dihedral angle between the two benzene rings is 1.6 (1)°. The mol­ecule adopts an E configuration with respect to the C=N double bond. An intra­molecular O—H⋯O hydrogen bond is observed. The Schiff base and methanol mol­ecules are linked into a two-dimensional network parallel to (10) by inter­molecular N—H⋯O, O—H⋯N and O—H⋯O hydrogen bonds.

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