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Eclipsed exocyclic carbon-oxygen bonds in the hexamethyl ether ofscyllo-inositol. X-ray crystallographic and NMR studies

Authors
Journal
Carbohydrate Research
0008-6215
Publisher
Elsevier
Publication Date
Volume
272
Issue
2
Identifiers
DOI: 10.1016/0008-6215(95)00090-g
Keywords
  • Eclipsed Exocyclic Carbon-Oxygen Bonds
  • Hexa Methyl Ether
  • Scyllo-Inositol

Abstract

Abstract Hexa- O-methyl- scyllo-inositol was synthesized and its crystal structure was determined by X-ray diffraction. As predicted by calculations, each oxygen-methyl bond eclipses the adjacent carbon-hydrogen bond. NMR studies show that the same conformation predominates in solution.

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