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Synthesis and properties of fullerene (C60) substituted cyclophosphazene derivatives

Authors
Journal
Inorganic Chemistry Communications
1387-7003
Publisher
Elsevier
Identifiers
DOI: 10.1016/j.inoche.2014.09.006
Keywords
  • Cyclotriphosphazene
  • Fullerene
  • Nmr
  • Fluorescence

Abstract

Abstract A series of fullerene (C60) substituted cyclophosphazene derivatives (2a–4a) were synthesized for the first time by 1,3-dipolar cycloaddition of the 1-formylphenoxy (aryloxy)cyclotriphosphazenes (2–4) (aryloxy=phenoxy, 1-naphthoxy and 1-pyrenoxy) and C60. All the obtained compounds were characterized by 1H NMR, 13C NMR, 31P NMR, UV–Vis, fluorescence spectroscopy, MALDI-TOF and elemental analysis. The thermal behaviors of the synthesized compounds were investigated by Thermal Gravimetric Analysis (TGA).

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