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3-Hy­droxy-8-oxo-3-nor-methyl­chamigrane-2,7-peroxide

Authors
Journal
Acta Crystallographica Section E Structure Reports Online
1600-5368
Publisher
International Union of Crystallography
Publication Date
Volume
66
Issue
7
Identifiers
DOI: 10.1107/s1600536810024517
Keywords
  • Organic Papers

Abstract

In the title compound, C14H22O4 (systematic name: 9-hy­droxy-1,5,5-trimethyl-1,8-epidi­oxy­spiro­[5.5]decan-2-one), which was isolated from the fermentation broth of Steccherinum ochraceum, the two six-membered rings adopt chair conformations and are bridged by a peroxide group. The hy­droxy H atom forms a three-centre cyclic inter­molecular O—H⋯(O,O′) hydrogen-bonding inter­action with a peroxide and a carbonyl O-atom acceptor, forming [100] chains.

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