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2-(1,3-Dithian-2-yl-idene)-1-phenyl-butane-1,3-dione.

Authors
  • 1
  • 1 College of Chemistry and Chemical Engineering, Liaoning Normal University, Dalian 116029, People's Republic of China. , (China)
Type
Published Article
Journal
Acta Crystallographica Section E Structure Reports Online
1600-5368
Publisher
International Union of Crystallography
Publication Date
Volume
64
Issue
Pt 2
Identifiers
DOI: 10.1107/S160053680800264X
PMID: 21201553
Source
Medline
License
Unknown

Abstract

The title compound, C(13)H(12)O(2)S(2), belonging to the group of dioxoketene cyclic S,S-acetals, was prepared from the corresponding dione in high yield. In the structure, the C=O and C=C bonds are not coplanar, with O=C-C=C torsion angles of -36.8 (4) and -21.0 (4)°. The dithian ring has a twisted conformation.

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