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1,10-Phenanthrolinium 2,3,4,5,6-penta-fluoro-benzoate-2,3,4,5,6-penta-fluoro-benzoic acid (1/2).

Authors
  • Zhang, Xiangdong
  • Men, Yanmei
  • Yan, Xianghua
  • Ge, Chunhua
  • Kong, Yuxia
Type
Published Article
Journal
Acta Crystallographica Section E Structure Reports Online
Publisher
International Union of Crystallography
Publication Date
Jan 01, 2009
Volume
65
Issue
Pt 10
Identifiers
DOI: 10.1107/S160053680903801X
PMID: 21577979
Source
Medline
License
Unknown

Abstract

In the title compound, C(12)H(9)N(2) (+)·C(7)F(5)O(2) (-)·2C(7)HF(5)O(2), the cation and anion are linked by an N-H⋯O hydrogen bond. The neutral mol-ecules bond to the anion via O-H⋯O hydrogen bonds to form associations of one cation, one anion and two neutral mol-ecules. Inter-molecular C-H⋯O, C-H⋯F, F⋯F [shortest contact = 2.768 (8) Å], F⋯π [shortest contact = 3.148 (13) Å] and π-π [shortest centroid-centroid separation = 3.689 (5) Å] inter-actions further link the components to form a three-dimensional network.

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