Affordable Access

Publisher Website

Preparation and characterization of electrodeposited amorphous molybdenum sulfide

Authors
Journal
Synthetic Metals
0379-6779
Publisher
Elsevier
Publication Date
Volume
29
Identifiers
DOI: 10.1016/0379-6779(89)90900-4
Keywords
  • Iii. Inorganic Polymers And Graphite Intercalation Compounds
Disciplines
  • Chemistry

Abstract

Abstract Amorphous molybdenum sulfide has been electrodeposited onto tin oxide-coated glass electrode from an aqueous ammonium tetrathiomolybdate solution. Cyclic voltammetry, potential step experiments, chemical analysis and scanning electron microscopy (SEM) have been used to characterize the deposited films. Cyclic voltammetry performed in the electrolytic bath, with and without supporting electrolyte, show that the oxidation of MoS 4 2− is completely irreversible. SEM micrographs of the deposited films indicate that the morphologies are thickness independent at high magnification but that cracks are clearly visible at lower magnification for thicker films.

There are no comments yet on this publication. Be the first to share your thoughts.

Statistics

Seen <100 times
0 Comments

More articles like this

Preparation and characterization of electrodeposit...

on Surface and Coatings Technolog... Jan 01, 1987

Preparation and characterization of amorphous mang...

on Materials Research Bulletin Jan 01, 2007

Preparation and characterization of molybdenum sul...

on Applied Catalysis A General Jan 01, 2006
More articles like this..