Hu, Tianliang Chen, Run Wang, Qiang He, Chiyang Liu, Shaorong
Published in
Journal of separation science
Sample pretreatment is essential for the analysis of complicated real samples due to their complex matrices and low analyte concentrations. Among all sample pretreatment methods, solid-phase extraction is arguably the most frequently used one. However, the majority of available solid-phase extraction adsorbents suffer from limited selectivity. Mole...
Welke, Juliane Elisa Hernandes, Karolina Cardoso Nicolli, Karine Primieri Barbará, Janaína Aith Biasoto, Aline Camarão Telles Zini, Claudia Alcaraz
Published in
Journal of separation science
The human nose has been used as a detector in gas chromatography analysis to evaluate odoriferous compounds related to aroma and quality of wine. Several olfactometric techniques are available to access the description, intensity, and/or duration of the odor of each compound. Olfactometry can be associated with one-dimensional gas chromatography or...
Kim, Un-Jung Karthikraj, Rajendiran
Published in
Journal of separation science
Sample preparation is one of the crucial steps in the analytical chemistry including human biomonitoring studies. Although there are several traditional approaches available, solid-phase microextraction is emerged as one of the pioneering techniques due to its simplicity, rapidness, wide applicability, and miniaturization of traditional sample prep...
Li, Congdi Chen, Zenglong Qin, Dongmei Liu, Rong Li, Li Li, Wei He, Yujian Yuan, Longfei
Published in
Journal of separation science
Tracing the herbicide bixlozone and its metabolites in food is necessary to assess their risks to human health. In the study, a rapid and effective analytical method using the quick, easy, cheap, effective, rugged, and safe (QuEChERS) method for the simultaneous determination of bixlozone and its metabolites (2,4-dichlorobenzoic acid, 3-hydroxy-pro...
Gao, Yang Wu, Yi Liu, Shu Liu, Zhiqiang Song, Fengrui Liu, Zhongying
Published in
Journal of separation science
Quickly identification the complex composition of traditional Chinese medicine only through liquid-mass spectrometry technology is difficult. Especially the identification of isomers and co-eluting compounds is even more difficult. In this study, an approach of multidimensional data modes based on an ultra-performance liquid chromatography coupled ...
Yang, Dongyue Wang, Songrui Huang, Xuhua Ma, Wenjuan Xue, Zixiang Zhao, Lulu Ouyang, Huizi He, Jun
Published in
Journal of separation science
A sensitive ultra-high performance liquid chromatography-tandem mass spectrometry method was developed and validated to clarify pharmacokinetic properties of 15 compounds (quercetin, isorhamnetin, chlorogenic acid, isoquercitrin, caffeic acid, scopoletin, 7-hydroxycoumarin, shionone, ferulic acid, kaempferol-7-O-β-D-glucopyranoside, methyl caffeate...
Torabi, Raheleh Rezvanipour, Abbas Ali Heiat, Mohammad
Published in
Journal of separation science
In a recent study conducted by Zhang et al. (2019), the adenosine monophosphate-specific aptamer has been applied for the rapid extraction of ochratoxin A. Although several publications have already reported the selection of adenosine monophosphate, adenosine triphosphate, and adenosine, there is no report on the detection of ochratoxin A using thi...
da Silva, Luis Felipe Lanças, Fernando Mauro
Published in
Journal of separation science
β-Cyclodextrin, coupled to graphene oxide supported on aminopropyl silica, was synthesized and characterized. This material was combined with microextraction by packed sorbent to act as the sample preparation step. The analytical method optimization was carried out by employing experimental design and had its figures of merit determined. The result...
Zacharias, Adway O Fang, Zixiang Rahman, Aurchie Talukdar, Akash Cornelius, Sharel Chowdhury, Saiful M
Published in
Journal of separation science
Protein posttranslational modifications and protein interactions are the central research areas in mass-spectrometry-based proteomics. Protein posttranslational modifications affect protein structures, stabilities, activities, and all cellular processes are achieved by interactions among proteins and protein complexes. With the continuing advanceme...
Li, Shuang Tang, Xinyi Lu, Yingying Xu, Jilin Chen, Juanjuan Chen, Haimin
Published in
Journal of separation science
Carotenoids consists of a series of conjugated isoprene units that are characteristically highly conjugated through double bonds, leading to the formation of many isomers that are susceptible to oxidation and other chemical modifications. Extreme hydrophobicity and high complexity make carotenoids difficult to identify and quantify. We implemented ...